Characterization of phenolic resins with thermogravimetry-mass spectrometry

Characterization of recycled mushroom compost leachate by chemical analysis and thermogravimetry-mass spectrometry.

Recycled compost leachate (RCL or euphemistically named "goody water") can be a potent source of foul odor on mushroom substrate production sites and contributes to composting smells. A complex mixture of sulfur compounds, fatty acids, and nitrogen containing compounds is responsible for odor production. Fifty samples, collected from 14 compost production sites in Ireland and the U.K. over a 2 ...

Characterization of Phenolic Resins and Their Co-Cure with Other Matrix Resins

Fractionation and characterization of phenolic resins by high-performance liquid chromatography and gel-permeation chromatography combined with ultraviolet, refractive index, mass spectrometry and light-scattering detection.

HPLC and gel permeation chromatographic (GPC) characterization of complex phenol-formaldehyde resins is described. Reversed-phase HPLC fingerprints the phenolic monomers, dimers and some oligomers. The molecular masses of these phenolic compounds were determined using an ion trap mass spectrometer. GPC analyzes tetrahydrofuran-soluble phenolic polymers beyond HPLC capability. The molecular mass...

Mechanistic and Kinetic Analysis of Na2SO4-Modified Laterite Decomposition by Thermogravimetry Coupled with Mass Spectrometry

Nickel laterites cannot be effectively used in physical methods because of their poor crystallinity and fine grain size. Na2SO4 is the most efficient additive for grade enrichment and Ni recovery. However, how Na2SO4 affects the selective reduction of laterite ores has not been clearly investigated. This study investigated the decomposition of laterite with and without the addition of Na2SO4 in...

Characterization of Environmentally Sustainable Resole Phenolic Resins Synthesized with Plant-based Bioresources

“Green” resole phenolic resins for laminating applications were synthesized, and their properties and thermal stability were determined. The plant-based cardanol and condensed tannin were used as the partial substitutes of up to 40% of the phenol in the synthesis of the phenolic resins. The resins were synthesized with different proportions of phenol (P) to cardanol (C) and with different total...